참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Aluminum sec-butoxide | HCID 61289 | — |
| 반응물 | 3,10-Dihexylpentacene-5,12-dione | HCID 22269484 | — |
| 용매 | Cyclohexanol | HCID 7966 | — |
| 생성물 | 2,9-Dihexylpentacene | HCID 17973372 | — |
반응 단계
A mixture of 5.69 grams of aluminum tri(sec-butoxide) and 49.1 mLs of cyclohexanol was made. To this was added 2.21 grams 3,10-Dihexylpentacene-5,12-dione. The reaction mixture was heated to 145° C. for 24 hours. The mixture was cooled to room temperature and the solid isolated by centrifugation. The solid was stirred with 40 mLs of cyclohexanol and centrifuged two times. The solid was collected by filtration and washed with THF to give 2,9-dihexylpentacene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06974877B2 |
|---|
| 출처 데이터셋 | uspto-grants-2005_12 |
|---|
| ORD ID | ord-6f4cfd59a8d54b509d5f65523dcba468 |
|---|
| 출처 메모 | uspto-grants-2005_12 |
|---|
