Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → 3-Hydroxy-2-iodo-1,6-dimethylpyridinium iodide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | 2-Iodo-6-methylpyridin-3-ol | HCID 89957 | — |
| 생성물 | 3-Hydroxy-2-iodo-1,6-dimethylpyridinium iodide | HCID 22266466 | — |
반응 단계
2-Iodo-3-hydroxy-6-methylpyridine (835 mg) and iodomethane (3 mL) were added in glass sealed cube, and the reaction mixture was reacted at 130° C. for 4 h and at 180° C. for 1 h. The reaction mixture was completely evaporated to give 3-hydroxy-2-iodo-1,6-dimethylpyridinium iodide (2-014-02) (1.42 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06977266B2 |
| 출처 데이터셋 | uspto-grants-2005_12 |
| ORD ID | ord-d943319b98874778abf70dda17c69d65 |
| 출처 메모 | uspto-grants-2005_12 |