참여 물질
| 역할 | 이름 | HCID | 투입량 |
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| 반응물 | Methylamine | HCID 6329 | — |
| 반응물 | (2S)-(4E)-5-(3-pyridyl)-4-penten-2-ol p-toluenesulfonate | HCID 87465994 | — |
| 생성물 | (2R)-(4E)-N-Methyl-5-(3-pyridyl)-4-penten-2-amine | HCID 9898976 | — |
반응 단계
A mixture of (2S)-(4E)-5-(3-pyridyl)-4-penten-2-ol p-toluenesulfonate (3.80 g, 11.97 mmol) and methylamine (20 mL, 2.0M solution in THF) was heated at 100-110° C. for 8 h in a sealed glass tube. The mixture was cooled to ambient temperature and concentrated under reduced pressure on a rotary evaporator. The resulting brown syrup was diluted with saturated NaHCO3 solution (25 mL) and extracted with chloroform (4×25 mL). The combined chloroform extracts were dried (K2CO3), filtered, and concentrated by rotary evaporation to afford a thick, brown syrup (2.00 g). The crude product was purified by column chromatography on silica gel, eluting with chloroform-methanol (95:5, v/v). Selected fractions were combined, concentrated by rotary evaporation affording a 800 mg (37.9%) of a pale-yellow oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US06979695B2 |
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| 출처 데이터셋 | uspto-grants-2005_12 |
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| ORD ID | ord-c1f47da3d71b446ca9c2f525bf45ecc5 |
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| 출처 메모 | uspto-grants-2005_12 |
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