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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 4908생성일: 2026년 10월 24일

Methanol → methyl 2-[(4,6-dimethoxytriazin-2-y1)oxy]-6-[1-(N-methoxyimino)ethyl]benzoate

https://huagongshe.com/ko/reaction/4908

반응식

참여 물질

역할이름HCID투입량
반응물MethanolHCID 887—
반응물Potassium AcetateHCID 517044—
반응물O-Methylhydroxylamine hydrochlorideHCID 521874—
반응물Methyl 2-acetyl-6-[(4,6-dimethoxytriazin-2-yl)oxy]benzoateHCID 19089388—
용매WaterHCID 962—
생성물methyl 2-[(4,6-dimethoxytriazin-2-y1)oxy]-6-[1-(N-methoxyimino)ethyl]benzoateHCID 8674718648%

반응 단계

0.9 of methyl 2-acetyl-6-[(4,6-dimethoxytriazin-2-yl)oxy]benzoate, 0.68 g of methoxyamine hydrochloride and 0.80 g of potassium acetate were added to 30 ml of methanol, and the resultant mixture was stirred for one day and one night at room temperature. The resultant reaction liquor was poured into water, and was extracted with ethyl acetate. After washing the extracted product with water, the washed product was dried and concentrated to obtain an oily product. This was then purified by column chromatography to obtain 0.47 g of the aimed compound (melting point=131° to 135° C.) at a yield of 48%.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05242895
출처 데이터셋uspto-grants-1993_09
ORD IDord-9caf7f2af9b04e69903afed00c9e43d0
출처 메모uspto-grants-1993_09