Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl Bromide → Diethyl 3-Bromobenzylphosphonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl Bromide | HCID 6332 | — |
| 반응물 | Triethyl phosphite | HCID 31215 | — |
| 반응물 | 3-Bromobenzyl bromide | HCID 69979 | — |
| 생성물 | Diethyl 3-Bromobenzylphosphonate | HCID 10979718 | — |
반응 단계
50 g (0.2 mol) of 3-bromobenzyl bromide and 33.2 g (0.2 mol) of triethyl phosphite were heated at 140° C. for 2 hours, during which ethyl bromide was distilled off. The product was distilled over a 30 cm Vigreux column.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05242908 |
| 출처 데이터셋 | uspto-grants-1993_09 |
| ORD ID | ord-5f68bfe24502413aa07932d4095cc464 |
| 출처 메모 | uspto-grants-1993_09 |