Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
o-Xylyl bromide → Diisopropyl 2-methylbenzylphosphonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | o-Xylyl bromide | HCID 6992 | — |
| 반응물 | Triisopropyl phosphite | HCID 8304 | — |
| 생성물 | Diisopropyl 2-methylbenzylphosphonate | HCID 15166402 | — |
반응 단계
34.5 g (0.19 mol) of 2-methylbenzyl bromide and 39 g (0.19 mol) of triisopropyl phosphite were heated at 150° C. for 2 hours. During this procedure, i-propyl bromide distilled off. The product was distilled through a 30 cm Vigreux column.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05242908 |
| 출처 데이터셋 | uspto-grants-1993_09 |
| ORD ID | ord-9bbd528effc4400bb7abc75186c3da13 |
| 출처 메모 | uspto-grants-1993_09 |