Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl Isothiocyanate → 4-Benzyl-2-(4-methoxybenzyl)-[1,2,4]thiadiazolidine-3,5-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl Isothiocyanate | HCID 2346 | — |
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | Isocyanic acid, p-methoxybenzyl- | HCID 187910 | — |
| 생성물 | 4-Benzyl-2-(4-methoxybenzyl)-[1,2,4]thiadiazolidine-3,5-dione | HCID 11602336 | — |
반응 단계
Reagents: Benzylisothiocyanate (6.5 mmol, 0.85 mL), p-metoxybenzyl-isocyanate (6.5 mmol, 0.92 mL) and SO2Cl2 (6.5 mmol, 0.52 mL) in diethyl ether (25 mL). Isolation: solvent evaporation. Purification: silica gel column chromatography (AcOEt/hexane, 1:4).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07531561B2 |
| 출처 데이터셋 | uspto-grants-2009_05 |
| ORD ID | ord-4e52b385adcd42919837a9ef2abb0606 |
| 출처 메모 | uspto-grants-2009_05 |