Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl Isothiocyanate → 4-Benzyl-2-(4-phenoxyphenyl)-[1,2,4]thiadiazolidine-3,5-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl Isothiocyanate | HCID 2346 | — |
| 반응물 | Diethyl Ether | HCID 3283 | — |
| 반응물 | 4-Phenoxyphenyl isocyanate | HCID 2734896 | — |
| 생성물 | 4-Benzyl-2-(4-phenoxyphenyl)-[1,2,4]thiadiazolidine-3,5-dione | HCID 11660810 | — |
반응 단계
Reagents: Benzylisothiocyanate (13 mmol, 1.6 mL), 4-phenoxyphenyl-isocyanate (13 mmol, 2.3 mL) and SO2Cl2 (13 mmol, 1 mL) in diethyl ether (50 mL). Isolation: filtration of reaction mixture. Purification: recrystallization from EtOH.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07531561B2 |
| 출처 데이터셋 | uspto-grants-2009_05 |
| ORD ID | ord-1267abc383c241faa1c8921cb0508a4d |
| 출처 메모 | uspto-grants-2009_05 |