Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Nitrobenzamide → 3-Nitrobenzylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Nitrobenzamide | HCID 12576 | — |
| 반응물 | Aluminium lithium hydride | HCID 21226445 | — |
| 생성물 | 3-Nitrobenzylamine | HCID 122722 | — |
반응 단계
Commercially available 3-nitrobenzamide is reduced with LAH under standard conditions to afford (3-nitrophenyl)methanamine, which is reacted with succinic anhydride under standard conditions to afford 1-(3-nitrobenzyl)pyrrolidine-2,5-dione. This material is reduced at the nitro group and oxidized to afford 1-(3-hydrazinobenzyl)pyrrolidine-2,5-dione.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07531566B2 |
| 출처 데이터셋 | uspto-grants-2009_05 |
| ORD ID | ord-6bdfe517728348d49aa48d175d29dc41 |
| 출처 메모 | uspto-grants-2009_05 |