Phenylphosphonic Acid → HCID 21506410, 화합물

HRID 492039

반응식

HRID 492039 반응식
[C:1]1([P:7](=[O:10])([OH:9])[OH:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[OH-].[Mg+2:12].[OH-]>O>[C:1]1([P:7](=[O:8])([O-:10])[O-:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Mg+2:12]

참가 물질

4

반응물 2

HCID 15295Phenylphosphonic AcidHCID 73981Magnesium Hydroxide

생성물 1

HCID 21506410HCID 21506410, 화합물수율 99%

시약·촉매·용매 1

HCID 962Water용매

반응 조건

온도
80 °C

실험 절차

1.58 g (10.0 mmol) of phenylphosphonic acid (manufactured by Nissan Chemical industries, Ltd.), 0.583 g (10.0 mmol) of magnesium hydroxide and 41 g of water were mixed, stirred at 80° C. for 3 hours, then water was distilled off under reduced pressure and dried at 200° C. to obtain 1.78 g (yield 99%) of the aimed product as white crystal. Decomposition temperature: 524° C.

후처리

  1. distillationwater was distilled off under reduced pressure
  2. customdried at 200° C.

출처 및 근거

ORD 기록
ord-c57a87bc93e14e7fbbb1c2c9a1a8f65f
출처 데이터셋
uspto-grants-2009_05
특허 번호
US07531585B2

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