참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Phenylphosphonic Acid | HCID 15295 | — |
| 반응물 | Zinc acetate (USP) | HCID 2724192 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Phosphonic acid, P-phenyl-, zinc salt (1:1) | HCID 15878909 | 98% |
반응 단계
1.58 g (10.0 mmol) of phenylphosphonic acid (manufactured by Nissan Chemical industries, Ltd.), 2.20 g (10.0 mmol) of zinc acetate dihydrate and 72 g of water were mixed, stirred at 80° C. for 3 hours, then the resulting slurry was filtered, acetic acid in the wet cake was fully washed away with water, and thereafter, dried at 150° C. to obtain 2.17 g (yield 98%) of the aimed product as white crystal. Decomposition temperature: 541° C. The average particle diameter was 4.4 μm with a laser diffraction type particle size distribution meter (manufactured by Seishin Enterprise Co., Ltd., PRO-7000S).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US07531585B2 |
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| 출처 데이터셋 | uspto-grants-2009_05 |
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| ORD ID | ord-29dd15cb096b4b0da85919b35f5415b0 |
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| 출처 메모 | uspto-grants-2009_05 |
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