Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tetrahydrothiophene → 1-(3,3-Dimethyl-2-oxobutyl)thiolan-1-ium bromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tetrahydrothiophene | HCID 1127 | — |
| 반응물 | Bromopinacolone | HCID 21642 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 1-(3,3-Dimethyl-2-oxobutyl)thiolan-1-ium bromide | HCID 22564578 | — |
반응 단계
70.2 Parts of tetrahydrothiophene was dissolved in 750 parts of acetone, and 150 parts of 1-bromo-3,3-dimethyl-2-butanone was added dropwise thereto. After the mixture was stirred at room temperature for 24 hours, white solid obtained was filtered, washed with acetone and dried to obtain 161.3 parts of 1-(3,3-dimethyl-2-oxobutyl)tetrahydrothiophenium bromide in the form of white crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07531686B2 |
| 출처 데이터셋 | uspto-grants-2009_05 |
| ORD ID | ord-4efe8ae645ce4c51b6e4a7eaecb65e22 |
| 출처 메모 | uspto-grants-2009_05 |