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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 492266생성일: 2026년 10월 26일

Tetrahydrothiophene → 1-(3,3-Dimethyl-2-oxobutyl)thiolan-1-ium bromide

https://huagongshe.com/reaction/492266

반응식

참여 물질

역할이름HCID투입량
반응물TetrahydrothiopheneHCID 1127—
반응물BromopinacoloneHCID 21642—
용매AcetoneHCID 180—
생성물1-(3,3-Dimethyl-2-oxobutyl)thiolan-1-ium bromideHCID 22564578—

반응 단계

70.2 Parts of tetrahydrothiophene was dissolved in 750 parts of acetone, and 150 parts of 1-bromo-3,3-dimethyl-2-butanone was added dropwise thereto. After the mixture was stirred at room temperature for 24 hours, white solid obtained was filtered, washed with acetone and dried to obtain 161.3 parts of 1-(3,3-dimethyl-2-oxobutyl)tetrahydrothiophenium bromide in the form of white crystals.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07531686B2
출처 데이터셋uspto-grants-2009_05
ORD IDord-4efe8ae645ce4c51b6e4a7eaecb65e22
출처 메모uspto-grants-2009_05