Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → N'-[(2'-nitro-1,1'-biphenyl-4-yl)methyl]-N'-pentyl-N-(2,4,6-trifluorophenyl)urea
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | P,P-Diphenylphosphinic azide | HCID 199401 | — |
| 반응물 | 2,4,6-Trifluorobenzoic acid | HCID 520373 | — |
| 반응물 | N-[(2'-nitro-1,1'-biphenyl-4-yl)methyl]-N-pentylamine | HCID 17860716 | — |
| 생성물 | N'-[(2'-nitro-1,1'-biphenyl-4-yl)methyl]-N'-pentyl-N-(2,4,6-trifluorophenyl)urea | HCID 68850802 | 95% |
반응 단계
Using 2,4,6-trifluorobenzoic acid (0.43 g), diphenylphosphoryl azide (0.68 g), triethylamine (0.25 g) and N-[(2′-nitro-1,1′-biphenyl-4-yl)methyl]-N-pentylamine (0.40 g), N′-[(2′-nitro-1,1′-biphenyl-4-yl)methyl]-N′-pentyl-N-(2,4,6-trifluorophenyl)urea (0.60 g) was obtained by a similar procedure as in Example 4. Yield: 95%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07531576B2 |
| 출처 데이터셋 | uspto-grants-2009_05 |
| ORD ID | ord-ad60fc8c99314aac82cf2db2c0b61c60 |
| 출처 메모 | uspto-grants-2009_05 |