Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Pentyne → 2-(Benzyloxy)-6-(2-n-propylethynyl)naphthalene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Pentyne | HCID 12309 | — |
| 반응물 | Trimethylsilylacetylene | HCID 66111 | — |
| 반응물 | 2-(Benzyloxy)-6-bromonaphthalene | HCID 640595 | — |
| 생성물 | 2-(Benzyloxy)-6-(2-n-propylethynyl)naphthalene | HCID 22925806 | — |
반응 단계
The reaction was conducted in the same manner as in the step (i) of the Example 31, except for using 2-(benzyloxy)-6-bromonaphthalene synthesized in the step (i) and 1-n-pentyne instead of 1-bromo-4-n-propylbenzene and trimethylsilylacetylene, respectively. The resultant was recrystallized from ethanol to give 2-(benzyloxy)-6-(2-n-propylethynyl)naphthalene.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07534547B2 |
| 출처 데이터셋 | uspto-grants-2009_05 |
| ORD ID | ord-5f136b0ba30b4f178ad1f7d0f9a890a6 |
| 출처 메모 | uspto-grants-2009_05 |