Methyl 1,2,3-benzothiadiazole-5-carboxylate → 1,2,3-Benzothiadiazole-5-carbaldehyde

HRID 493119

반응식

HRID 493119 반응식
[S:1]1[C:5]2[CH:6]=[CH:7][C:8]([C:10](OC)=[O:11])=[CH:9][C:4]=2[N:3]=[N:2]1>[O-2].[Mn+2]>[S:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH:10]=[O:11])=[CH:9][C:4]=2[N:3]=[N:2]1

참가 물질

3

반응물 1

HCID 2736813Methyl 1,2,3-benzothiadiazole-5-carboxylate

생성물 1

HCID 185046971,2,3-Benzothiadiazole-5-carbaldehyde

시약·촉매·용매 1

HCID 160959Manganese oxide촉매

실험 절차

This was prepared from methyl benzo[1,2,3]thiadiazole-5-carboxylate (0.291 g) by the method of Example 16c, (except that the alcohol was stirred with manganese (II) oxide overnight) and used without purification.

후처리

  1. customused without purification

출처 및 근거

ORD 기록
ord-678b3452850d437296836a9f87966be9
출처 데이터셋
uspto-grants-2009_05
특허 번호
US07534793B2

연결된 노트

불러오는 중…