Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Fluoro-6-nitroaniline → 3-Fluorobenzene-1,2-diamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Fluoro-6-nitroaniline | HCID 87316 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 3-Fluorobenzene-1,2-diamine | HCID 2782835 | — |
반응 단계
A solution of 2-fluoro-6-nitro-phenylamine [K. L. Kirk and L. A. Cohen J. Org. Chem. 34, 384-389 (1969)] (1.05 g) in ethanol (50 ml) was hydrogenated over 10% palladium on carbon (0.5 g), filtered and evaporated to give a brown solid, used without purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07534793B2 |
| 출처 데이터셋 | uspto-grants-2009_05 |
| ORD ID | ord-c493ca06571448c0add5b9ae3bca65e2 |
| 출처 메모 | uspto-grants-2009_05 |