Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,2-Benzenedicarboxylic acid, 4-nitro- → 4-Aminophthalic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,2-Benzenedicarboxylic acid, 4-nitro- | HCID 69121 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 4-Aminophthalic acid | HCID 72912 | — |
반응 단계
1 g (4.73 mmol) of 4-nitrophthalic acid is dissolved in 10 mL of anhydrous ethanol. The solution is stirred at room temperature and degassed under argon. 50 mg of palladium/charcoal (5%) are added in a single portion and hydrogen is bubbled into the solution. After 3 hours, the solution is filtered through Celite and then evaporated.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06706725B1 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-d56bdbc58160413788ea7d8ded70198f |
| 출처 메모 | uspto-grants-2004_03 |