참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-(2-Naphthoxy)ethanol | HCID 7131 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | 2,3-Dichloropyrazine | HCID 78575 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | 2-Chloro-3-[2-(2-naphthyloxy)ethoxy]pyrazine | HCID 23509565 | — |
반응 단계
Sodium hydride (55% dispersion in mineral oil; 44 mg, 1.0 mmol) was added to a mixture of 2-(2-naphthoxy)ethanol (188 mg, 1.00 mmol) and 2,3-dichloropyrazine (149 mg, 1.00 mmol) in dioxane (0.5 mL), and the reaction mixture was stirred at 40° C. for 15 h. The crude material was used directly in Step 2.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07534794B2 |
|---|
| 출처 데이터셋 | uspto-grants-2009_05 |
|---|
| ORD ID | ord-bfed6779a35d4e33a019655fe10f3cc9 |
|---|
| 출처 메모 | uspto-grants-2009_05 |
|---|
