Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → 4-Ethoxycarbonylphenylboronic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 4-Carboxyphenylboronic Acid | HCID 312183 | — |
| 생성물 | 4-Ethoxycarbonylphenylboronic acid | HCID 2734350 | — |
반응 단계
A solution of 4-carboxyphenylboronic acid (15 g, 0.09 mol), 99% ethanol (150 mL) and concentrated sulphuric acid (0.5 mL) was heated to reflux for two days. The volume was reduced to approximately 20 mL. The residue was triturated with petroleum ether to give 13.4 g of the desired material.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06706749B2 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-bf48985882e84c38afed626b7b44b7a8 |
| 출처 메모 | uspto-grants-2004_03 |