Methyl 2-allyl-2-phenyl-4-pentenoate → Methyl 2-(4-fluorophenyl)-2-propylpentanoate

HRID 494476노트

반응식

HRID 494476 반응식
[CH2:1]([C:4]([C:12]1[CH:17]=[CH:16][C:15]([F:18])=[CH:14][CH:13]=1)([CH2:9][CH:10]=[CH2:11])[C:5]([O:7][CH3:8])=[O:6])[CH:2]=[CH2:3].C(C(C1C=CC=CC=1)(CC=C)C(OC)=O)C=C>>[F:18][C:15]1[CH:14]=[CH:13][C:12]([C:4]([CH2:9][CH2:10][CH3:11])([CH2:1][CH2:2][CH3:3])[C:5]([O:7][CH3:8])=[O:6])=[CH:17][CH:16]=1

참가 물질

3

반응물 2

HCID 11085592Methyl 2-allyl-2-phenyl-4-pentenoateHCID 68872335Methyl 2-allyl-2-(4-fluorophenyl)pent-4-enoate

생성물 1

HCID 68873955Methyl 2-(4-fluorophenyl)-2-propylpentanoate

실험 절차

The title compound was prepared according to the procedure of Example 1B, substituting the compound of Example 14B for the compound of Example 1A. 1H NMR (300 MHz, CDCl3): δ 0.89 (t, J=6.99 Hz, 6 H) 1.07 (m, 4 H) 1.95 (m, 4 H) 3.63 (s, 3 H) 6.99 (t, J=8.64 Hz, 2 H) 7.22 (m, 2 H).

출처 및 근거

ORD 기록
ord-bec03b789ef645cc81bab42a24e955de
출처 데이터셋
uspto-grants-2009_05
특허 번호
US07538105B2

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