참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Carbazole | HCID 6854 | — |
| 반응물 | Boron trifluoride etherate | HCID 8000 | — |
| 용매 | Acetic Anhydride | HCID 7918 | — |
| 생성물 | 9-Acetyl-9H-carbazole | HCID 95837 | — |
반응 단계
Carbazole (100.24 g) was suspended in acetic anhydride (300 mL) with catalytic boron trifluoride etherate (0.65 mL) and the solution refluxed for 25 min. then cooled to 0° C. and the solid was then collected and recrystallized from hexane to give 82.65 g 9-acetyl-carbazole.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06706753B2 |
|---|
| 출처 데이터셋 | uspto-grants-2004_03 |
|---|
| ORD ID | ord-5daec04b8dd84e07a58c039f40a8ecf2 |
|---|
| 출처 메모 | uspto-grants-2004_03 |
|---|
