Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium Carbonate → 4-Hydroxyisophthalic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium Carbonate | HCID 10340 | — |
| 반응물 | 4-Bromo-1,3-benzenedicarboxylic acid | HCID 81361 | — |
| 생성물 | 4-Hydroxyisophthalic acid | HCID 12490 | 82% |
반응 단계
The same procedure as described in Example 24 was performed but using 2.45 g (10.0 mmol) of 4-bromoisophthalic acid as the substrate and 2.70 g (25.5 mmol) of Na2CO3 instead of Ca(OH)2. A total of 1.49 g (8.2 mmol, 82% yield) of 4-hydroxyisophthalic acid was collected. The purity was determined by 1H NMR to be 88%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07538244B2 |
| 출처 데이터셋 | uspto-grants-2009_05 |
| ORD ID | ord-5acdf371e6a04f0ea8b33c454fcfb52f |
| 출처 메모 | uspto-grants-2009_05 |