Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Nitrodiphenylamine → N-Phenyl-o-phenylenediamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Nitrodiphenylamine | HCID 8407 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | N-Phenyl-o-phenylenediamine | HCID 68297 | — |
반응 단계
To a pressure reaction bottle was added 10 g 2-nitrodiphenylamine, 0.5 g 5% palladium on carbon and 100 ml 95% ethanol. The mixture was hydrogenated at 22 C and 40 psi hydrogen for 2 hours. Following filtration through celite and solvent removal, an oil was obtained that crystallized on standing.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07538931B2 |
| 출처 데이터셋 | uspto-grants-2009_05 |
| ORD ID | ord-0d005ecc997b4d5fbe48d7c073be4aec |
| 출처 메모 | uspto-grants-2009_05 |