Methyl 2-(1-methylpiperidin-4-ylidene)acetate → Methyl 2-(1-methylpiperidin-4-yl)acetate

HRID 495482노트

반응식

HRID 495482 반응식
[CH3:1][O:2][C:3](=[O:12])[CH:4]=[C:5]1[CH2:10][CH2:9][N:8]([CH3:11])[CH2:7][CH2:6]1>[Pd].CCO>[CH3:1][O:2][C:3](=[O:12])[CH2:4][CH:5]1[CH2:6][CH2:7][N:8]([CH3:11])[CH2:9][CH2:10]1

참가 물질

4

반응물 1

HCID 20672702Methyl 2-(1-methylpiperidin-4-ylidene)acetate

생성물 1

HCID 19425952Methyl 2-(1-methylpiperidin-4-yl)acetate

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 702Ethanol용매

실험 절차

(1-Methyl-piperidin-4-ylidene)-acetic acid methyl ester (Step A) was stirred under H2 overnight (1.1 g of 10% Pd/C and 200 mL EtOH), filtered and evaporated to give (1-methyl-piperidin-4-yl)-acetic acid methyl ester as a yellow oil/white solid.

후처리

  1. filtrationfiltered
  2. customevaporated

출처 및 근거

ORD 기록
ord-dacca3ed436b4d0f94be5b29df70d83f
출처 데이터셋
uspto-grants-2005_09
특허 번호
US06939874B2

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