Cyclohexene → HCID 69796510, 화합물

HRID 495604노트

반응식

HRID 495604 반응식
C(OC([N:11]1[CH2:15][CH2:14][CH2:13][C@@H:12]1[CH2:16][O:17][Si:18]([C:21]([CH3:24])([CH3:23])[CH3:22])([CH3:20])[CH3:19])=O)C1C=CC=CC=1.C1CCCCC=1>C(O)C.[Pd]>[Si:18]([O:17][CH2:16][C@H:12]1[CH2:13][CH2:14][CH2:15][NH:11]1)([C:21]([CH3:24])([CH3:23])[CH3:22])([CH3:20])[CH3:19]

참가 물질

5

반응물 2

HCID 8079CyclohexeneHCID 14629888HCID 14629888, 화합물

생성물 1

HCID 69796510HCID 69796510, 화합물수율 86.3%

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 702Ethanol용매

실험 절차

To a solution of D2 (12.7 g, 0.036 mol) and cyclohexene (excess, 20 ml) in ethanol (100 ml) was added 10% palladium on charcoal catalyst. Reaction was heated at reflux overnight and cooled. Catalyst was filtered and the filtrate concentrated to leave an oil (6.69 g) which was used in the next step without purification.

후처리

  1. customReaction
  2. temperaturewas heated
  3. temperatureat reflux overnight
  4. temperaturecooled
  5. filtrationCatalyst was filtered
  6. concentrationthe filtrate concentrated

출처 및 근거

ORD 기록
ord-aa3eccba618748809eeaaf288611ce69
출처 데이터셋
uspto-grants-2005_09
특허 번호
US06939891B2

반응 노트

불러오는 중…