돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 495613생성일: 2026년 10월 25일

Ethyl 2-chlorophenyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamate → Ethyl 2-chlorophenyl[2,4-diamino-6-(trifluoromethyl)phenyl]carbamate

https://huagongshe.com/reaction/495613

반응식

참여 물질

역할이름HCID투입량
반응물Ethyl 2-chlorophenyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamateHCID 20827737—
촉매PalladiumHCID 23938—
용매Ethyl AcetateHCID 8857—
생성물Ethyl 2-chlorophenyl[2,4-diamino-6-(trifluoromethyl)phenyl]carbamateHCID 2082773698%

반응 단계

Ethyl 2-chlorophenyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamate (0.645 g) was dissolved in ethyl acetate (100 ml), and to the solution was added 10% Pd—C (0.58 g). The reaction mixture was stirred under hydrogen atmosphere for 11 hours. The catalyst was filtered, and washed with ethyl acetate. The filtrate and washing were combined and concentrated in vacuo to give the title compound (0.543 g, 98%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06939887B2
출처 데이터셋uspto-grants-2005_09
ORD IDord-55614f05576d45bc80a182b2496dd400
출처 메모uspto-grants-2005_09