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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 495619생성일: 2026년 10월 26일

Ethyl 2-chlorobenzyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamate → Ethyl 2-chlorobenzyl[2,4-diamino-6-(trifluoromethyl)phenyl]carbamate

https://huagongshe.com/reaction/495619

반응식

참여 물질

역할이름HCID투입량
반응물Ethyl 2-chlorobenzyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamateHCID 20827734—
촉매PalladiumHCID 23938—
용매Ethyl AcetateHCID 8857—
생성물Ethyl 2-chlorobenzyl[2,4-diamino-6-(trifluoromethyl)phenyl]carbamateHCID 2082773395.2%

반응 단계

Ethyl 2-chlorobenzyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamate (103.8 mg) was dissolved in ethyl acetate (20 ml), and to the solution was added 10% Pd—C (105.3 mg). The reaction mixture was stirred under hydrogen atmosphere for 7 hours. The catalyst was filtered, and washed with ethyl acetate. The filtrate was concentrated in vacuo to give the title compound (85.6 mg).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06939887B2
출처 데이터셋uspto-grants-2005_09
ORD IDord-42b2cb5cb8b84dfab453a2c3b421b67a
출처 메모uspto-grants-2005_09