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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 495627생성일: 2026년 10월 26일

Ethyl 4-chlorobenzyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamate → Ethyl 4-chlorobenzyl[2,4-diamino-6-(trifluoromethyl)phenyl]carbamate

https://huagongshe.com/reaction/495627

반응식

참여 물질

역할이름HCID투입량
반응물Ethyl 4-chlorobenzyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamateHCID 20827746—
촉매PalladiumHCID 23938—
용매Ethyl AcetateHCID 8857—
생성물Ethyl 4-chlorobenzyl[2,4-diamino-6-(trifluoromethyl)phenyl]carbamateHCID 2082774597.4%

반응 단계

Ethyl 4-chlorobenzyl[2,4-dinitro-6-(trifluoromethyl)phenyl]carbamate (294.7 mg) was dissolved in ethyl acetate (20 ml), and to the solution was added 10% Pd—C (267.7 mg). The reaction mixture was stirred under hydrogen atmosphere for 7 hours. The catalyst was filtered, and washed with ethyl acetate. The filtrate was concentrated in vacuo to give the title compound (248.7 mg).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06939887B2
출처 데이터셋uspto-grants-2005_09
ORD IDord-22e9506486f448879edec20695904024
출처 메모uspto-grants-2005_09