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Malic Acid → Dicalciumhydroxy malate

HRID 49640
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HRID 49640 반응식
[OH-:1].[Ca+2:2].[OH-].[C:4]([OH:12])(=[O:11])[CH:5]([CH2:7][C:8]([OH:10])=[O:9])[OH:6]>O>[C:4]([O:12][OH:1])(=[O:11])[CH:5]([CH2:7][C:8]([O-:10])=[O:9])[OH:6].[Ca+2:2].[Ca+2:2].[OH:1][O:11][C:4](=[O:12])[CH:5]([CH2:7][C:8]([O-:10])=[O:9])[OH:6].[OH:1][O:11][C:4](=[O:12])[CH:5]([CH2:7][C:8]([O-:10])=[O:9])[OH:6].[OH:1][O:11][C:4](=[O:12])[CH:5]([CH2:7][C:8]([O-:10])=[O:9])[OH:6]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 525Malic AcidHCID 6093208Calcium Hydroxide

생성물 1

HCID 86594317Dicalciumhydroxy malate

시약·촉매·용매 1

HCID 962Water용매6회

실험 절차

A dicalciumhydroxy malate granular product was prepared by mixing two molar equivalents of particulate calcium hydroxide with one molar equivalent of particulate malic acid (totaling 45 kg for the entire composition) in a Ribbon Blender for 15 minutes at normal speeds. A water jacket was used to ensure that the product would not over react when small amounts of water were added to the batch. Next, about 1 L of water was slowly sprayed into the particulate mixture product. After about 10 minutes of reaction time (where the product became spongy and had risen, and then dropped back to a more granular state), an additional 1 L of water was added. This was repeated several times until no further reaction appeared to be occurring upon addition of water. The end result was a granular product. Once a fully reacted granular product was formed, no additional water was added. The resulting composition was then dried in a cool room and ground to a predetermined particle size.

후처리

  1. customfor 15 minutes
  2. additionwere added to the batch
  3. customAfter about 10 minutes of reaction time (where the product
  4. additionwas added
  5. customuntil no further reaction
  6. customThe end result
  7. customOnce a fully reacted granular product was formed
  8. customThe resulting composition was then dried in a cool room and ground to a predetermined particle size

출처 및 근거

ORD 기록
ord-8769067acfb941b59d1328669d86bb6a
출처 데이터셋
uspto-grants-2004_03
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US06706904B1

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