Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium hydride → ethyl 4-[benzyl-(4-methoxybenzenesulfonyl)amino]-1-phenyl-1H-pyrazolo[3,4-b]pyridine-5-carboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | N-benzyl-4-methoxybenzenesulfonamide | HCID 741351 | — |
| 반응물 | Ethyl 4-chloro-1-phenyl-1H-pyrazolo[3,4-b]pyridine-5-carboxylate | HCID 3572813 | — |
| 생성물 | ethyl 4-[benzyl-(4-methoxybenzenesulfonyl)amino]-1-phenyl-1H-pyrazolo[3,4-b]pyridine-5-carboxylate | HCID 22322147 | — |
반응 단계
Following the procedure of Example 35, the product of Example 33 is reacted with benzyl-(4-methoxybenzenesulfonyl)amine and sodium hydride to provide ethyl 4-[benzyl-(4-methoxybenzenesulfonyl)amino]-1-phenyl-1H-pyrazolo[3,4-b]pyridine-5-carboxylate. m.p. 124°-126° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06946473B2 |
| 출처 데이터셋 | uspto-grants-2005_09 |
| ORD ID | ord-bf3726e4ec3240e4b230c7bc1c413611 |
| 출처 메모 | uspto-grants-2005_09 |