참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | 1-Chloroanthraquinone | HCID 6709 | — |
| 반응물 | Tetraethylene Glycol | HCID 8200 | — |
| 생성물 | 1-[2-[2-[2-(2-Hydroxyethoxy)ethoxy]ethoxy]ethoxy]-9,10-anthraquinone | HCID 22315914 | — |
반응 단계
A mixture of 1-chloroanthraquinone (4 gm) potassium carbonate, (4 gm) in tetraethyleneglycol (15 ml) was heated for three hours at 120° C., poured into cool water and filtered off. The solid obtained was chromatographed over silica gel and eluted with methylene chloride:methanol (99:1) gave 1-[2-[2-[2-(2-hydroxyethoxy)ethoxy]ethoxy]ethoxy]-9,10-anthraquinone. This compound was crystallized from ether to give a yellow crystalline compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06949250B2 |
|---|
| 출처 데이터셋 | uspto-grants-2005_09 |
|---|
| ORD ID | ord-5eed529334914c5fb74af65902f2fd7b |
|---|
| 출처 메모 | uspto-grants-2005_09 |
|---|
