Triethylamine → tert-Butyl 3-aminopropanoate

HRID 497007

반응식

HRID 497007 반응식
Cl.[C:2]([O:6][C:7](=[O:11])[CH2:8][CH2:9][NH2:10])([CH3:5])([CH3:4])[CH3:3].C(N(CC)CC)C>C(Cl)Cl>[C:2]([O:6][C:7](=[O:11])[CH2:8][CH2:9][NH2:10])([CH3:5])([CH3:4])[CH3:3]

참가 물질

4

반응물 2

HCID 8471TriethylamineHCID 16218890Tert-butyl 3-aminopropanoate hydrochloride

생성물 1

HCID 4192171tert-Butyl 3-aminopropanoate

시약·촉매·용매 1

HCID 6344Dichloromethane용매

실험 절차

To a solution of β-alanine t-butyl ester hydrochloride (5 mmol, SIGMA) in CH2Cl2 (20 mL) was added triethylamine (5 mmol) at RT After the solution was stirred at RT for 15 mins, the precipitate formed was filtered and the CH2Cl2 was removed in vacuo to give the free amine, β-alanine t-butyl ester.

후처리

  1. customthe precipitate formed
  2. filtrationwas filtered
  3. customthe CH2Cl2 was removed in vacuo

출처 및 근거

ORD 기록
ord-0b961f3abcdd4277846e8487a30e5a18
출처 데이터셋
uspto-grants-2005_09
특허 번호
US06949534B2

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