Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Toluene → alpha-Methylstyrene isopropenyltoluene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Toluene | HCID 1140 | — |
| 반응물 | Alpha-Methylstyrene | HCID 7407 | — |
| 반응물 | O,alpha-dimethylstyrene | HCID 81886 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | alpha-Methylstyrene isopropenyltoluene | HCID 86585334 | — |
반응 단계
250 g α-methyl styrene (99.8% purity), 250 g isopropenyltoluene, and 500 g toluene were introduced into a three-mouthed flask, and mixed while boron trifluoride phenol complex was slowly added, and the material was then cooled under dry ice and acetone solvent and reacted for 3 hr at 20° C. Next, alkali was added to inactivate and remove the catalyst, and concentrated to remove the solvent and unreacted monomer, and α-methylstyrene-isopropenyltoluene copolymer was obtained as a residue. This polymer was designated Polymer B3, and its physical properties are listed in Table 2.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06709798B2 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-db5f8f3c860240cb9161dd66c55b5231 |
| 출처 메모 | uspto-grants-2004_03 |