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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 498204생성일: 2026년 10월 26일

[5-(Methyl-propyl-amino)-2-nitro-4-trifluoromethyl-phenyl]-carbamic acid tert-butyl ester → Carbamic acid,[2-amino-5-(methylpropylamino)-4-(trifluoromethyl)phenyl]-,1,1-dimethylethyl ester

https://huagongshe.com/reaction/498204

반응식

참여 물질

역할이름HCID투입량
반응물[5-(Methyl-propyl-amino)-2-nitro-4-trifluoromethyl-phenyl]-carbamic acid tert-butyl esterHCID 69487144—
촉매PalladiumHCID 23938—
생성물Carbamic acid,[2-amino-5-(methylpropylamino)-4-(trifluoromethyl)phenyl]-,1,1-dimethylethyl esterHCID 69486655—

반응 단계

The title compound was prepared from [5-(methyl-propyl-amino)-2-nitro-4-trifluoromethyl-phenyl]-carbamic acid tert-butyl ester (Example C5) (3.78 g, 10.0 mmol) by hydrogenation with 10% Pd/C according to the general procedure J (method a). Obtained as a red oil (3.40 g, 98%).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06949542B2
출처 데이터셋uspto-grants-2005_09
ORD IDord-9f8e75c493db45df88d0c26740e94504
출처 메모uspto-grants-2005_09