Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
(4-Methyl-2-nitro-5-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester → (2-Amino-4-methyl-5-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | (4-Methyl-2-nitro-5-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester | HCID 69486805 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | (2-Amino-4-methyl-5-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester | HCID 69489396 | 87% |
반응 단계
Prepared from (4-methyl-2-nitro-5-trifluoromethyl-phenyl)-carbamic acid tert-butyl ester (Example A18) (4.68 g, 14.6 mmol) by hydrogenation with 10% Pd/C according to the general procedure J (method a). Obtained as a white solid (3.68 g, 87%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06949542B2 |
| 출처 데이터셋 | uspto-grants-2005_09 |
| ORD ID | ord-43be8b0323224b32b648ee39f67ac3ca |
| 출처 메모 | uspto-grants-2005_09 |