Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
L-Leucine, N-((1,1-dimethylethoxy)carbonyl)- → Boc-Leu-Gly-Leu-Ala-OBzl
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | L-Leucine, N-((1,1-dimethylethoxy)carbonyl)- | HCID 83170 | — |
| 반응물 | H-Gly-Leu-Ala-OBzl | HCID 131717745 | — |
| 생성물 | Boc-Leu-Gly-Leu-Ala-OBzl | HCID 131717746 | — |
반응 단계
Boc-Leu-Gly-Leu-Ala-OBzl was prepared by coupling Boc-Leu-OH (2.62 g, 10.5 mmoles) to H-Gly-Leu-Ala-OBzl using the mixed anhydride procedure described in Example 2. The resulting product was crystallized from ethyl acetate:hexane to yield 2.7 g (mp 95°-96°) in the first crop.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05242904 |
| 출처 데이터셋 | uspto-grants-1993_09 |
| ORD ID | ord-dcb3efb5c2714b649c6024418e3d449a |
| 출처 메모 | uspto-grants-1993_09 |