Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HCID 67530783, 화합물 → HCID 67529444, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | HCID 67530783 | HCID 67530783 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 촉매 | Platinum oxide monohydrate | HCID 86587499 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 67529444 | HCID 67529444 | — |
반응 단계
This compound was prepared in a manner analogous to that of Step E of Example 1, by the hydrogenation of 0.5 gram (0.0022 mole) of 3-(imidazol-5-yl)-5-methoxy-6-methylindene (viii) in the presence of 0.1 gram (catalyst) of 10% palladium on carbon and 0.1 gram (catalyst) of platinum oxide hydrate in 40 mL of ethanol. The yield of subject compound was 0.42 gram, mp 68-70° C. The NMR spectrum was consistent with the proposed structure.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07767667B2 |
| 출처 데이터셋 | uspto-grants-2010_08 |
| ORD ID | ord-ddef700dccce4e6487c6d9dacbbe1683 |
| 출처 메모 | uspto-grants-2010_08 |