참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | 1,4-Dioxane | HCID 31275 | — |
| 반응물 | 6-Quinolinecarboxylic acid | HCID 82571 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | 6-Quinolinecarboxylic acid, ethyl ester | HCID 94670 | — |
반응 단계
4.9 g of quinoline-6-carboxylic acid was stirred in 80 ml of ethanol. 40 ml of dioxane containing 4 M of hydrogen chloride was added to the obtained mixture. After stirring at 70° C. overnight, the solvent was evaporated and the residue was treated with ethyl acetate as the extracting solvent by an ordinary method to obtain the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06710056B2 |
|---|
| 출처 데이터셋 | uspto-grants-2004_03 |
|---|
| ORD ID | ord-39bdd5917a824cf489af4d15fa464529 |
|---|
| 출처 메모 | uspto-grants-2004_03 |
|---|
