Ammonia → HCID 178512765, 화합물

HRID 49934

반응식

HRID 49934 반응식
[NH2:1][CH2:2][C:3]1[CH:11]=[CH:10][C:6]([C:7]([OH:9])=[O:8])=[CH:5][CH:4]=1.N.[N:13]#[C:14][NH2:15]>O>[NH:1]([CH2:2][C:3]1[CH:4]=[CH:5][C:6]([C:7]([OH:9])=[O:8])=[CH:10][CH:11]=1)[C:14]([NH2:15])=[NH:13]

참가 물질

5

반응물 3

HCID 222AmmoniaHCID 9864CyanamideHCID 655264-(Aminomethyl)Benzoic Acid

생성물 1

HCID 178512765HCID 178512765, 화합물

시약·촉매·용매 1

HCID 962Water용매

반응 조건

온도
60 °C

실험 절차

A mixture of 1.51 g (10.0 mmol) of 4-aminomethylbenzoic acid, 20 ml of water, 2.0 ml of 28% aqueous ammonia and 1.00 g (23.8 mmol) of cyanamide was stirred at 60° C. overnight. The white precipitate thus formed was taken by the filtration, washed with water and dried to obtain the title compound.

후처리

  1. customThe white precipitate thus formed
  2. filtrationwas taken by the filtration
  3. washwashed with water
  4. customdried

출처 및 근거

ORD 기록
ord-c887df8de4df4a55a09c1569fe4de64f
출처 데이터셋
uspto-grants-2004_03
특허 번호
US06710056B2

연결된 노트

불러오는 중…