돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 49940생성일: 2026년 10월 24일

Tetrahydrofuran → (1,1'-Biphenyl)-3-carboxylic acid

https://huagongshe.com/ko/reaction/49940

반응식

참여 물질

역할이름HCID투입량
반응물TetrahydrofuranHCID 8028—
반응물Sodium HydroxideHCID 14798—
반응물Methyl 3-phenylbenzoateHCID 9855857—
용매MethanolHCID 887—
생성물(1,1'-Biphenyl)-3-carboxylic acidHCID 12854—

반응 단계

0.90 g of methyl 3-phenylbenzoate was fed into 20 ml of a solvent mixture of aqueous solution of 2 M of sodium hydroxide, tetrahydrofuran and methanol (4/2/1) to conduct the reaction at 70° C. for 2 hours. The solvent was evaporated, and the residue was fed into 3 M of hydrochloric acid. The precipitate thus formed was taken by the filtration and dried to obtain the title compound in the form of white crystals.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US06710056B2
출처 데이터셋uspto-grants-2004_03
ORD IDord-b6d106859ae042a0be8637cd84cd0072
출처 메모uspto-grants-2004_03