Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tetrahydrofuran → (1,1'-Biphenyl)-3-carboxylic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tetrahydrofuran | HCID 8028 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Methyl 3-phenylbenzoate | HCID 9855857 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | (1,1'-Biphenyl)-3-carboxylic acid | HCID 12854 | — |
반응 단계
0.90 g of methyl 3-phenylbenzoate was fed into 20 ml of a solvent mixture of aqueous solution of 2 M of sodium hydroxide, tetrahydrofuran and methanol (4/2/1) to conduct the reaction at 70° C. for 2 hours. The solvent was evaporated, and the residue was fed into 3 M of hydrochloric acid. The precipitate thus formed was taken by the filtration and dried to obtain the title compound in the form of white crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06710056B2 |
| 출처 데이터셋 | uspto-grants-2004_03 |
| ORD ID | ord-b6d106859ae042a0be8637cd84cd0072 |
| 출처 메모 | uspto-grants-2004_03 |