Potassium Carbonate → HCID 22939443, 화합물
반응식
C([O:4][CH2:5][CH2:6][CH2:7][C:8]1[CH:13]=[CH:12][CH:11]=[C:10]([C:14]#[N:15])[N:9]=1)(=O)C.C(=O)([O-])[O-].[K+].[K+]>CO>[OH:4][CH2:5][CH2:6][CH2:7][C:8]1[N:9]=[C:10]([C:14]#[N:15])[CH:11]=[CH:12][CH:13]=1참가 물질
4
실험 절차
3-(6-Cyano-2-pyridyl)propyl acetate (3.0 g, 14.7 mmol) was dissolved in methanol (15 ml), and potassium carbonate (0.08 g, 0.58 mmol) was added thereto. The reaction mixture was stirred at room temperature for 22 hrs and concentrated to give the titled compound (2.2 g, 92%).
후처리
- concentrationconcentrated
출처 및 근거
- ORD 기록
- ord-bb9bf859fb124a6eb520b64cc2685f74
- 출처 데이터셋
- uspto-grants-2010_08
- 특허 번호
- US07767665B2
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