HCID 22939353, 화합물 → HCID 59750359, 화합물

반응식

C([O:8][C:9]1[N:14]=[C:13]([C:15]2[S:16][C:17]3[CH:25]=[CH:24][CH:23]=[CH:22][C:18]=3[C:19](=[O:21])[N:20]=2)[CH:12]=[CH:11][CH:10]=1)C1C=CC=CC=1>FC(F)(F)C(O)=O>[O:8]=[C:9]1[NH:14][C:13]([C:15]2[S:16][C:17]3[CH:25]=[CH:24][CH:23]=[CH:22][C:18]=3[C:19](=[O:21])[N:20]=2)=[CH:12][CH:11]=[CH:10]1

참가 물질

실험 절차

2-(6-(Benzyloxy)-2-pyridyl)-4H-1,3-benzothiazine-4-one (0.15 g, 0.43 mmol) was dissolved in trifluoroacetic acid (10 ml), and the mixture was stirred at room temperature for 15 hrs. The solvent was evaporated, and the residue was recrystallized from chloroform-hexane to give the titled compound (0.07 g, 69%).

후처리

customThe solvent was evaporated
customthe residue was recrystallized from chloroform-hexane

출처 및 근거

ORD 기록: ord-21742255427b4962affbdcf27c0acfa8
출처 데이터셋: uspto-grants-2010_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07767665B2

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참가 물질

반응물 1

HCID 22939353HCID 22939353, 화합물

생성물 1

HCID 59750359HCID 59750359, 화합물수율 69%

시약·촉매·용매 1

HCID 6422Trifluoroacetic acid용매

실험 절차

후처리

customThe solvent was evaporated
customthe residue was recrystallized from chloroform-hexane

출처 및 근거

ORD 기록: ord-21742255427b4962affbdcf27c0acfa8
출처 데이터셋: uspto-grants-2010_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07767665B2

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불러오는 중…