Methacrylic anhydride → HCID 86615999, 화합물

HRID 499946

반응식

HRID 499946 반응식
[CH3:1][CH:2]([OH:13])[CH2:3][O:4][CH:5]([CH2:7][O:8][CH:9]([CH2:11][OH:12])[CH3:10])[CH3:6].[C:14]([O:19]C(=O)C(C)=C)(=[O:18])[C:15]([CH3:17])=[CH2:16]>O1CCCC1>[C:14]([OH:19])(=[O:18])[C:15]([CH3:17])=[CH2:16].[CH3:1][CH:2]([OH:13])[CH2:3][O:4][CH:5]([CH2:7][O:8][CH:9]([CH2:11][OH:12])[CH3:10])[CH3:6]

참가 물질

4

반응물 2

HCID 12974Methacrylic anhydrideHCID 326112-(2-(2-Hydroxypropoxy)propoxy)-1-propanol

생성물 1

HCID 86615999HCID 86615999, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

In a 0.5 L separable flask, 0.1 mol of tripropylene glycol and 0.1 mol of methacrylic anhydride were mixed in anhydrous tetrahydrofuran. After stirring the mixture for a while, the internal pressure of the container was reduced to volatile the content and the material was distilled off to obtain tripropylene glycol monomethacrylate.

후처리

  1. distillationthe material was distilled off

출처 및 근거

ORD 기록
ord-2eaa2d1a4fd143a79701feee30e9cbde
출처 데이터셋
uspto-grants-2010_08
특허 번호
US07767753B2

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