Methacrylic anhydride → Tripropylene glycol monomethacrylate
반응식
[CH3:1][CH:2]([OH:13])[CH2:3][O:4][CH:5]([CH2:7][O:8][CH:9]([CH2:11][OH:12])[CH3:10])[CH3:6].[C:14]([O:19]C(=O)C(C)=C)(=[O:18])[C:15]([CH3:17])=[CH2:16]>O1CCCC1>[C:14]([OH:19])(=[O:18])[C:15]([CH3:17])=[CH2:16].[CH3:1][CH:2]([OH:13])[CH2:3][O:4][CH:5]([CH2:7][O:8][CH:9]([CH2:11][OH:12])[CH3:10])[CH3:6]참가 물질
4
실험 절차
In a 0.5 L separable flask, 0.1 mol of tripropylene glycol and 0.1 mol of methacrylic anhydride were mixed in anhydrous tetrahydrofuran. After stirring the mixture for a while, the internal pressure of the container was reduced to volatile the content and the material was distilled off to obtain tripropylene glycol monomethacrylate.
후처리
- distillationthe material was distilled off
출처 및 근거
- ORD 기록
- ord-2eaa2d1a4fd143a79701feee30e9cbde
- 출처 데이터셋
- uspto-grants-2010_08
- 특허 번호
- US07767753B2
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