Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
N,N'-di-sec-butylidene-4,4'-methylenebis(2,6-diethylbenzeneamine) → N,N'-di-sec-butyl-4,4'-methylenebis(2,6-diethylbenzeneamine)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | N,N'-di-sec-butylidene-4,4'-methylenebis(2,6-diethylbenzeneamine) | HCID 86608152 | — |
| 촉매 | Platinum | HCID 23939 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | N,N'-di-sec-butyl-4,4'-methylenebis(2,6-diethylbenzeneamine) | HCID 66781129 | — |
반응 단계
N,N′-di-sec-butylidene-4,4′-methylenebis(2,6-diethylbenzeneamine) (22.53 g) and Pt(S)/C (2.65 g) were added to acetone (34.0 g) in an autoclave. The closed autoclave was purged 3 times with 125 psig of H2 (9.63×105 Pa) at 22° C. The mixture was kept at 21° C. and 125 psi (8.62×105 Pa) of H2 for 6.5 hours, forming the corresponding N,N′-di-sec-butyl-4,4′-methylenebis(2,6-diethylbenzeneamine) quantitatively.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07767858B2 |
| 출처 데이터셋 | uspto-grants-2010_08 |
| ORD ID | ord-89a1f47fe05b44cb85f0618e9dc4766f |
| 출처 메모 | uspto-grants-2010_08 |