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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 501870생성일: 2026년 10월 26일

Acetic Acid → 2-Bromo-5-tert-butyl-1,3-dimethylbenzene

https://huagongshe.com/reaction/501870

반응식

참여 물질

역할이름HCID투입량
반응물Acetic AcidHCID 176—
반응물5-Tert-butyl-m-xyleneHCID 7378—
반응물BromineHCID 24408—
용매WaterHCID 962—
생성물2-Bromo-5-tert-butyl-1,3-dimethylbenzeneHCID 22036494.7%

반응 단계

Under an inert atmosphere, 225 g of acetic acid was put into a 500 ml three-necked flask, and 24.3 g of 5-t-butyl-m-xylene was added. Then, after adding 31.2 g of bromine, it was reacted at 15-20° C. for 3 hours. The reaction liquid was added to 500 ml of water, and the deposited precipitate was filtrated. It was washed with 250 ml of water twice and 34.2 g of white solid was obtained.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07772360B2
출처 데이터셋uspto-grants-2010_08
ORD IDord-bda8c24223b24e88ad61a1e994bf420d
출처 메모uspto-grants-2010_08