Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Acetic Acid → 2-Bromo-5-tert-butyl-1,3-dimethylbenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | 5-Tert-butyl-m-xylene | HCID 7378 | — |
| 반응물 | Bromine | HCID 24408 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 2-Bromo-5-tert-butyl-1,3-dimethylbenzene | HCID 220364 | 94.7% |
반응 단계
Under an inert atmosphere, 225 g of acetic acid was put into a 500 ml three-necked flask, and 24.3 g of 5-t-butyl-m-xylene was added. Then, after adding 31.2 g of bromine, it was reacted at 15-20° C. for 3 hours. The reaction liquid was added to 500 ml of water, and the deposited precipitate was filtrated. It was washed with 250 ml of water twice and 34.2 g of white solid was obtained.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07772360B2 |
| 출처 데이터셋 | uspto-grants-2010_08 |
| ORD ID | ord-bda8c24223b24e88ad61a1e994bf420d |
| 출처 메모 | uspto-grants-2010_08 |