1,6-Dioxaspiro[2.5]octane → HCID 59255059, 화합물

HRID 502895

반응식

HRID 502895 반응식
[C:1]([O:5][C:6](=[O:15])[NH:7][CH2:8][CH:9]1[CH2:14][CH2:13][NH:12][CH2:11][CH2:10]1)([CH3:4])([CH3:3])[CH3:2].[O:16]1[C:18]2([CH2:23][CH2:22][O:21][CH2:20][CH2:19]2)[CH2:17]1>CO>[C:1]([O:5][C:6](=[O:15])[NH:7][CH2:8][CH:9]1[CH2:10][CH2:11][N:12]([CH2:17][C:18]2([OH:16])[CH2:23][CH2:22][O:21][CH2:20][CH2:19]2)[CH2:13][CH2:14]1)([CH3:4])([CH3:2])[CH3:3]

참가 물질

4

반응물 2

HCID 1604391,6-Dioxaspiro[2.5]octaneHCID 723429Tert-butyl (piperidin-4-ylmethyl)carbamate

생성물 1

HCID 59255059HCID 59255059, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

To a stirred solution of tert-butyl(piperidin-4-ylmethyl)carbamate (22.3 g, 104 mmol) in methanol was added 1,6-dioxaspiro[2.5]octane (14.2 g, 124 mmol, Satyamurthy, Nagichettiar et al., Phosphorus Sulfur, 1984, 19, 113) at ambient temperature.

출처 및 근거

ORD 기록
ord-4915662e86cd4417b09f827755efa109
출처 데이터셋
uspto-grants-2010_08
특허 번호
US07776885B2

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