Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Sodium hydride → 1-(2-Thienyl)cyclopent-3-ene-1-carbonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | 2-Thienylacetonitrile | HCID 72880 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 1-(2-Thienyl)cyclopent-3-ene-1-carbonitrile | HCID 65353080 | — |
반응 단계
Thiophene-2-acetonitrile and 1,4-dichloride-2-butene were added to a DMF solution of sodium hydride washed with hexane and the whole was reacted at room temperature to obtain 1-(2-thienyl)cyclopent-3-ene-1-carbonitrile.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07776897B2 |
| 출처 데이터셋 | uspto-grants-2010_08 |
| ORD ID | ord-8008992ec5f640278445eefa7cfdca24 |
| 출처 메모 | uspto-grants-2010_08 |