참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 2-Methylhexanoic Acid | HCID 20653 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Hexanoic acid, 2-methyl-, methyl ester | HCID 519892 | 93% |
반응 단계
A solution of 2-methylhexanoic acid (20 g, 153 mmol) in methanol (500 mL) was treated with concentrated sulfuric acid (8.0 mL) and heated to 50° C. for 16 h. The reaction was diluted with water and extracted with ether. The combined organic layers were dried and concentrated to afford 20.57 g (93%) of methyl 2-methylhexanoate as a colorless liquid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07776896B2 |
|---|
| 출처 데이터셋 | uspto-grants-2010_08 |
|---|
| ORD ID | ord-dd7c0667478e4394b22e5f59ab7fce31 |
|---|
| 출처 메모 | uspto-grants-2010_08 |
|---|
