Copper carbonate → Copper Diammonium Bitetrazole

HRID 50513

반응식

HRID 50513 반응식
[N:1]1[C:5](=[C:6]2[N:10]=[N:9][N:8]=[N:7]2)[N:4]=[N:3][N:2]=1.[NH4+:11].[NH4+].C(=O)([O-])[O-].[Cu+2:17]>O>[N:1]1[C:5](=[C:6]2[N:10]=[N:9][N:8]=[N:7]2)[N:4]=[N:3][N:2]=1.[NH4+:11].[NH4+:1].[Cu+2:17]

참가 물질

4

반응물 2

HCID 14452Copper carbonateHCID 86588366Diammonium bitetrazole

생성물 1

HCID 86588365Copper Diammonium Bitetrazole

시약·촉매·용매 1

HCID 962Water용매

반응 조건

온도
90 °C

실험 절차

In this Example, 60.87 grams of diammonium bitetrazole were suspended in 120 ml of deionized water. Subsequently, 39.13 grams of basic copper carbonate were added to the reaction mixture. The resulting reaction mixture was heated to 90° C. and continued to be heated and stirred for approximately 1 hour. A solid was formed that was filtered, washed with water, filtered again and then vacuum oven dried at 80° C. The resulting solid was in a yield of 85.95 grams as compared to the theoretical yield of 83.86 grams. (NOTE: The greater than theoretical yield is believed attributable to incomplete conversion of the starting materials during processing.) TABLE 2, below, identifies the elemental chemical analysis of the material formed as well as the elemental chemical analysis for a corresponding theoretical composition of CuC2H6N10. The x-ray diffraction pattern obtained for a powder sample of the material of Example 2 is shown in FIG. 2.

후처리

  1. customThe resulting reaction mixture
  2. temperatureto be heated
  3. customA solid was formed
  4. filtrationthat was filtered
  5. washwashed with water
  6. filtrationfiltered again
  7. customvacuum oven dried at 80° C
  8. custom(NOTE: The greater than theoretical yield
  9. customformed as well as the elemental chemical analysis for a corresponding theoretical composition of CuC2H6N10

출처 및 근거

ORD 기록
ord-53dc2cbfb592404e950ee091dbe3f311
출처 데이터셋
uspto-grants-2004_03
특허 번호
US06712918B2

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