참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Dinitrofluorobenzene | HCID 6264 | — |
| 반응물 | N-methyl-2-pyrrolidone | HCID 13387 | — |
| 반응물 | 3-(Heptadecafluorooctyl)aniline | HCID 4245356 | — |
| 용매 | Triethylamine | HCID 8471 | — |
| 생성물 | N-[3-(perfluorooctyl)phenyl]-2,4-dinitrobenzenamine | HCID 22735001 | 83.2% |
반응 단계
A mixture of 3-(perfluoro-n-octyl)benzenamine (2.04 g), 2,4-dinitrofluorobenzene (0.78 g), NMP (8 mL) and triethylamine (0.85 mL) was heated to 70° C. for 16 hr. Extraction and recrystallization from hexane-ethyl acetate gave N-[3-(perfluorooctyl)phenyl]-2,4-dinitrobenzenamine (2.25 g, mp 124.5-125° C.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US06713135B2 |
|---|
| 출처 데이터셋 | uspto-grants-2004_03 |
|---|
| ORD ID | ord-9d2b141ac7a345f3a67ae2d06bc2c97c |
|---|
| 출처 메모 | uspto-grants-2004_03 |
|---|
